HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-[3-Methoxy-5-(pentafluorosulfanyl)phenyl]ethanone → 1-[3-Bromo-5-(pentafluorosulfanyl)phenyl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-[3-Methoxy-5-(pentafluorosulfanyl)phenyl]ethanone | HCID 44183118 | — |
| Reactant | 3-Bromo-N-methoxy-N-methyl-5-(pentafluorosulfanyl)benzamide | HCID 58137464 | — |
| Product | 1-[3-Bromo-5-(pentafluorosulfanyl)phenyl]ethanone | HCID 58137430 | — |
Reaction Steps
3-Bromo-N-methoxy-N-methyl-5-(pentafluorosulfanyl)benzamide (1.1 g) was converted and worked up analogously to 21d). Purification by means of HPLC was not necessary. 935 mg of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466169B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-0638a360c6e0479685fe10f5a85c7df0 |
| Source note | uspto-grants-2013_06 |