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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1258542Generated: October 30, 2026

M-Phenylenediamine → HCID 86640289, compound

https://huagongshe.com/reaction/1258542

Reaction equation

Participants

RoleNameHCIDCharge
ReactantM-PhenylenediamineHCID 7935—
ReactantHCID 17837208HCID 17837208—
ProductHCID 86640289HCID 86640289—

Reaction Steps

N-(3-Amino-phenyl)-2-methyl-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)-benzamide was prepared from benzene-1,3-diamine and 2-methyl-4-(1,2,2,2-tetrafluoro-1-trifluoromethyl-ethyl)-benzoyl chloride (Example I4) using the same procedure. 1H-NMR (CDCl3, 400 MHz): 7.6 (m, 1H), 7.52 (s, 2H), 7.40 (s, 1H), 7.30 (s, 1H), 7.13 (t, 1H), 6.72 (d, 1H), 6.50 (d, 1H), 3.76 (s, 2H), 2.24 (s, 3H) ppm.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08466180B2
Source datasetuspto-grants-2013_06
ORD IDord-4d1a728ad51e4b219fc7a2d971d84824
Source noteuspto-grants-2013_06