HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,1'-Thiocarbonyldi-2(1H)-pyridone → HCID 86646343, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,1'-Thiocarbonyldi-2(1H)-pyridone | HCID 853162 | — |
| Reactant | N-(3-amino-4-chlorobenzyl)pivalamide | HCID 66765386 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86646343 | HCID 86646343 | — |
Reaction Steps
1,1′-Thiocarbonyldi-2-pyridone (2.12 g, 9.1 mmol) was added to a mixture of N-(3-amino-4-chlorobenzyl)-2,2-dimethyl-propionamide (2.00 g, 8.3 mmol) and DCM (60 mL) and stirred at rt for 1.5 h. The mixture was filtered over silica gel. The organic layer was concentrated to give the sub-title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466186B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-7125d667e7ff480ebce03b54f597e544 |
| Source note | uspto-grants-2013_06 |