HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 178447318, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 178509819 | HCID 178509819 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178447318 | HCID 178447318 | — |
Reaction Steps
The sub-title compound was prepared from 3-[6-(5-aza-spiro[2.4]hept-5-yl)-5-chloro-1H-benzimidazol-2-ylamino]-4-chloro-benzylamine (60 mg, 0.1), pivaloyl chloride (20 μL, 0.1 mmol) and TEA (160 μL, 1.1 mmol) in THF (5 mL) in analogy to example 3, step (e).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466186B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-bc4a7eb800ef4e18be7c619db5aff167 |
| Source note | uspto-grants-2013_06 |