HuagongsheHuagongshe Chemistry Print Report · For research reference only
Pivaloyl chloride → HCID 178483241, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Pivaloyl chloride | HCID 62493 | — |
| Reactant | HCID 178483240 | HCID 178483240 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178483241 | HCID 178483241 | — |
Reaction Steps
The title compound was prepared analogously to example 3 step (e) from 4-chloro-3-[5-chloro-6-(2-dimethylaminomethyl-pyrrolidin-1-yl)-1H-benzimidazol-2-ylamino]-benzylamine (30 mg), pivaloyl chloride (10 μL, 0.06 mmol) and TEA (70 μL, 0.54 mmol) in THF (2 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466186B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-8a82ba121c964ca5a4d1301c7326a996 |
| Source note | uspto-grants-2013_06 |