HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 88532156, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 5-Chloro-2-nitro-4-(trifluoromethyl)aniline | HCID 2773813 | — |
| Reactant | 4-(Trifluoromethyl)piperidine hydrochloride | HCID 16218160 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 88532156 | HCID 88532156 | — |
Reaction Steps
The sub-title compound was prepared from 4-trifluoromethyl-5-chloro-2-nitro-aniline (100 mg, 0.42 mmol), 4-trifluoromethyl-piperidine hydrochloride (394 mg, 2.1 mmol) and K2CO3 (600 mg, 4.4 mmol) in NMP (2 mL) in analogy to example 3, step (a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08466186B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-532df4f6581e44258ac41db2445c898b |
| Source note | uspto-grants-2013_06 |