Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1259864Generated: November 3, 2026

Methanol → HCID 67204266, compound

https://huagongshe.com/reaction/1259864

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantHCID 67204263HCID 67204263—
ReactantHCID 178418361HCID 178418361—
CatalystHCID 178418390HCID 178418390—
SolventWaterHCID 962—
ProductHCID 67204266HCID 6720426685%

Reaction Steps

A suspension of 50% hydrated 10% palladium-carbon (180 mg) in water (1 mL) was added to a methanol (10 mL) solution of 2-(2-acetoxyphenyl)-4-quinolinecarboxylic acid benzyl ester (940 mg, 2.34 mmol) obtained above, and the mixture was stirred for 7 hours in a hydrogen atmosphere. The catalyst was filtered off through celite, and then, the solvent was distilled off to obtain the title compound (610 mg, 1.99 mmol).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08466290B2
Source datasetuspto-grants-2013_06
ORD IDord-32acab3cc7dd49e592b6444a60d803fd
Source noteuspto-grants-2013_06