HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(p-Nonylphenoxy)ethanol → Tergitol mesylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(p-Nonylphenoxy)ethanol | HCID 7700 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Sodium Tetradecyl Sulfate | HCID 23665772 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Tergitol mesylate | HCID 131730653 | — |
Reaction Steps
The Tergitol-mesylate was synthesized as depicted in Reaction Scheme 3 and FIG. 1. In step S1, 4.86 g (48 mmol) of triethylamine (Aldrich) was added to a solution of Tergitol®NP-9 (16 mmol, Aldrich) in anhydrous methylene chloride (20 ml) in a reactor. The mixture was stirred under a nitrogen atmosphere for 10 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470209B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-dad952767dde4a789f995cfa6f92a9cc |
| Source note | uspto-grants-2013_06 |