HRID1260124
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
The Tergitol-mesylate was synthesized as depicted in Reaction Scheme 3 and FIG. 1. In step S1, 4.86 g (48 mmol) of triethylamine (Aldrich) was added to a solution of Tergitol®NP-9 (16 mmol, Aldrich) in anhydrous methylene chloride (20 ml) in a reactor. The mixture was stirred under a nitrogen atmosphere for 10 minutes.
WORKUP
后处理
- customas depicted in Reaction Scheme 3 and FIG. 1