HRID1260165

反应详情

EQUATION

反应方程式

HRID 1260165 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

KMUP-1 (8.0 g) is dissolved in a mixture of ethanol (10 mL) and citric acid (4 g) and reacted at 50° C. for 20 min, the methanol is added thereinto under room temperature and the solution is incubated over night for crystallization and filtrated to obtain KMUP-1-Citric acid salt (10.5 g).

WORKUP

后处理

  1. customreacted at 50° C. for 20 min
  2. customunder room temperature and the solution is incubated over night for crystallization
  3. filtrationfiltrated