HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → KMUP-1 Citric acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Kmup 1 | HCID 10453764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | KMUP-1 Citric acid | HCID 49783485 | 88.9% |
Reaction Steps
KMUP-1 (8.0 g) is dissolved in a mixture of ethanol (10 mL) and citric acid (4 g) and reacted at 50° C. for 20 min, the methanol is added thereinto under room temperature and the solution is incubated over night for crystallization and filtrated to obtain KMUP-1-Citric acid salt (10.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470805B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-58696b869e9146ebb174ff76c9d355fb |
| Source note | uspto-grants-2013_06 |