HRID1260166
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
KMUP-1 (8.0 g) is dissolved in a mixture of ethanol (10 mL) and nicotinic acid (2.4 g) and reacted at 50° C. for 20 min, the methanol is added thereinto under room temperature and the solution is incubated over night for crystallization and filtrated to obtain KMUP-1-Nicotinic acid salt (8.3 g).
WORKUP
后处理
- customreacted at 50° C. for 20 min
- customunder room temperature and the solution is incubated over night for crystallization
- filtrationfiltrated