HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → KMUP-1 Nicotinic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Kmup 1 | HCID 10453764 | — |
| Solvent | Nicotinic Acid | HCID 938 | — |
| Product | KMUP-1 Nicotinic acid | HCID 51039835 | — |
Reaction Steps
KMUP-1 (8.0 g) is dissolved in a mixture of ethanol (10 mL) and nicotinic acid (2.4 g) and reacted at 50° C. for 20 min, the methanol is added thereinto under room temperature and the solution is incubated over night for crystallization and filtrated to obtain KMUP-1-Nicotinic acid salt (8.3 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470805B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-72f38d681114404db802a736be8234bd |
| Source note | uspto-grants-2013_06 |