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HRID1260467

反应详情

EQUATION

反应方程式

HRID 1260467 的结构方程式

REACTANTS

反应物

3
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：C1COCCO1
HCID31275

1,4-Dioxane

C4H8O2

结构：COC(=O)[C@@H]1CN(C(=O)OC(C)(C)C)CCN1C(=O)N[C@H]1C[C@@H]1c1ccccc1
HCID86656057

未命名化合物

PRODUCTS

生成物

1
结构：Cl.O=C1[C@@H]2CNCCN2C(=O)N1[C@H]1C[C@@H]1c1ccccc1
HCID67300061

未命名化合物

PROCEDURE

实验过程

4N HCl solution in dioxane (44 eq.) was added at RT to D1. The resulting 0.1 M solution obtained was stirred for 1 h at RT, then the solvent was removed under reduced pressure. The residue was co-evaporated with toluene (×3) and it was used as such in next step without further purification. MS (ES+) C15H17N3O2 requires 271, found: 272 (M+H)+.