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HRID1260493

反应详情

EQUATION

反应方程式

HRID 1260493 的结构方程式

REACTANTS

反应物

1
结构：CC(Oc1ccc(N2CCC3(CCN(Cc4ccccc4)CC3O)C2=O)cc1)C(F)(F)F
HCID58056626

未命名化合物

PRODUCTS

生成物

1
结构：CC(Oc1ccc(N2CCC3(CCNCC3O)C2=O)cc1)C(F)(F)F
HCID58056627

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：[OH-].[OH-].[Pd+2]
催化剂HCID9942167

Palladium hydroxide

H2O2Pd

PROCEDURE

实验过程

The title compound was prepared in analogy to example 2 step A from a mixture of (5 SR,6RS)-8-benzyl-6-hydroxy-2-[4-((rac)-2,2,2-trifluoro-1-methyl-ethoxy)-phenyl]-2,8-diaza-spiro[4.5]decan-1-one and Pearlman's catalyst under an atmosphere of hydrogen. Light brown solid. MS (ESI): 359.1 (MH+)