HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 178474770, compound → HCID 178474769, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 178474770 | HCID 178474770 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178474769 | HCID 178474769 | — |
Reaction Steps
cis-N-{3-[5-(4-Benzyloxyphenoxy)-[1,3]dioxan-2-yl]propyl}acetamide (25 mg, 0.065 mmol) was dissolved in 5 ml of ethanol and hydrogenated in the presence of 0.69 mg of palladium/carbon under 3 bar for 1 h. The reaction mixture was concentrated and directly reacted further. Yield 18 mg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-725d179ca8a04b649fc752bc0661d607 |
| Source note | uspto-grants-2013_06 |