HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-chloropyrimidine → HCID 86656065, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-chloropyrimidine | HCID 606665 | — |
| Reactant | 2-Chloro-5-hydroxypyridine | HCID 819821 | — |
| Product | HCID 86656065 | HCID 86656065 | — |
Reaction Steps
6-Chloropyridin-3-ol (670 mg, 5.17 mmol) and 5-bromo-2-chloropyrimidine (1.0 g, 5.17 mmol) were reacted in analogy to example 2c. Yield: 1.02 g (69%), M+H+: 285.95.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-eaab43ec051f47d68987a2f0f9429dbe |
| Source note | uspto-grants-2013_06 |