HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67071818, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86761883 | HCID 86761883 | — |
| Product | HCID 67071818 | HCID 67071818 | — |
Reaction Steps
tert-Butyl {2-[4-(5-isopropoxypyridin-2-yloxy)phenoxy]-1-methylethyl}carbamate (414 mg, 1.03 mmol) was treated with 90% strength trifluoroacetic acid for 4 h. The trifluoroacetic acid was distilled off and the aqueous phase was freeze dried. The crude product contains excess trifluoroacetic acid and was further reacted without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-9297748bf7c24bbd8325d591c5ac0c1c |
| Source note | uspto-grants-2013_06 |