HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-[3-(4-Hydroxyphenyl)-1-methylpropyl]acetamide → HCID 49858095, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-[3-(4-Hydroxyphenyl)-1-methylpropyl]acetamide | HCID 59956161 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Rhodium | HCID 23948 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 49858095 | HCID 49858095 | — |
Reaction Steps
N-[3-(4-Hydroxyphenyl)-1-methylpropyl]acetamide (1.0 g, 4.82 mmol) were dissolved in 100 ml of ethanol and hydrogenated in the presence of 5% rhodium on carbon (695 mg) at 100° C. and 100 bar hydrogen pressure for 18 h. The catalyst was filtered off and the filtrate was concentrated. Yield: 1.06 g of crude product, M+H+: 214.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-b016762b2f3047b5a1ce06c92fc13e19 |
| Source note | uspto-grants-2013_06 |