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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1260561Generated: November 1, 2026

Pyridine → HCID 86656071, compound

https://huagongshe.com/reaction/1260561

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPyridineHCID 1049—
ReactantBenzyloxyamine hydrochlorideHCID 102312—
ReactantHCID 67302610HCID 67302610—
SolventEthanolHCID 702—
ProductHCID 86656071HCID 86656071—

Reaction Steps

1-[4-(6-Isopropoxypyridin-3-yloxy)phenyl]-4-methylpentan-3-one (310 mg, 0.947 mmol) was stirred with O-benzylhydroxylamine hydrochloride (181 mg, 1.14 mmol) and pyridine (0.92 ml, 1.14 mmol) in 5 ml of ethanol at room temperature for 18 h. The reaction mixture was concentrated and further reacted without purification. Yield: 310 mg, M+H+: 433.26.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08470841B2
Source datasetuspto-grants-2013_06
ORD IDord-3925882072e3471a800518980c27e7ec
Source noteuspto-grants-2013_06