HuagongsheHuagongshe Chemistry Print Report · For research reference only
(E)-4-(4-Hydroxyphenyl)-3-buten-2-one → HCID 67071785, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (E)-4-(4-Hydroxyphenyl)-3-buten-2-one | HCID 796857 | — |
| Reactant | 2-Isopropoxy-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyridine | HCID 24208798 | — |
| Product | HCID 67071785 | HCID 67071785 | — |
Reaction Steps
2-Isopropoxy-5-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)pyridine (3.24 g, 12.33 mmol) and (E)-4-(4-hydroxyphenyl)but-3-en-2-one (2.0 g, 12.33 mmol) were reacted in analogy to example 50a. Yield: 304 mg (8%), M+H+: 298.2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470841B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-3947fff1a8f34076a2942a08e8bab04c |
| Source note | uspto-grants-2013_06 |