HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,3,3-Trifluoropropionic acid → HCID 178520719, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,3,3-Trifluoropropionic acid | HCID 2777972 | — |
| Reactant | HCID 178478590 | HCID 178478590 | — |
| Product | HCID 178520719 | HCID 178520719 | — |
Reaction Steps
The title compound, white solid (49 mg, 70%), MS (ISP) m/z=441.4 [(M+H)+], mp 216.5° C., was prepared in accordance with the general method of example 6 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (70.4 mg, 0.16 mmol) 3,3,3-trifluoropropanoic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470828B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-4220f30c342a4e0c8056f600f07c2e67 |
| Source note | uspto-grants-2013_06 |