HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methylisoxazole-5-carboxylic acid → HCID 178427119, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methylisoxazole-5-carboxylic acid | HCID 853085 | — |
| Reactant | HCID 178478590 | HCID 178478590 | — |
| Product | HCID 178427119 | HCID 178427119 | — |
Reaction Steps
The title compound, white solid (99 mg, 90%), MS (ISP) m/z=440.4 [(M+H)+], mp 199° C., was prepared in accordance with the general method of example 6 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and 3-methyl-isoxazole-5-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08470828B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-6b3922d101d0423f912b56b436b48966 |
| Source note | uspto-grants-2013_06 |