2,4-Dichlorobenzoic Acid → HCID 178523728, compound

Participants

Reaction Steps

The title compound, white solid (119 mg, 95%), MS (ISP) m/z=503.2 [(M+H)+], mp 243.5° C., was prepared in accordance with the general method of example 6 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and 2,4-dichloro-benzoic acid.

Provenance & Evidence