Dimethylcarbamoyl Chloride → HCID 178484726, compound

Participants

Reaction Steps

The title compound, white solid (81 mg, 81%), MS (ISP) m/z=402.5 [(M+H)+], mp 217.5° C., was prepared in accordance with the general method of example 26 from trans-4-{2-[4-(2,3-dihydro-furo[2,3-c]pyridin-7-yl)-piperazin-1-yl]-ethyl}-cyclohexylamine trihydrochloride (intermediate B) (110 mg, 0.25 mmol) and dimethylcarbamic acid chloride.

Provenance & Evidence