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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1261823Generated: November 2, 2026

Ethanol → HCID 68089168, compound

https://huagongshe.com/reaction/1261823

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthanolHCID 702—
ReactantHCID 51355076HCID 51355076—
SolventMethanolHCID 887—
ProductHCID 68089168HCID 6808916879%

Reaction Steps

In accordance with the method described in Example 6, except that 43.14 g (3S)-cyclohexyl 3-(tert-butoxycarbonylamino)-4-hydroxy-4-(2,4,5-trifluorophenyl)butyrate and an equal amount of anhydrous ethanol were used to replace (3S)-3-(tert-butoxycarbonylamino)-4-hydroxy-4-(2,4,5-trifluorophenyl)n-butyl ester and methanol respectively, 32.82 g (R)-cyclohexyl 3-(tert-butoxycarbonylamino)-4-(2,4,5-trifluorophenyl)butyrate (yield: 79%) was obtained using the same method.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08471057B2
Source datasetuspto-grants-2013_06
ORD IDord-ed20837efb30474897d504fafdcbc829
Source noteuspto-grants-2013_06