HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 66710773, compound → HCID 66711761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 66710773 | HCID 66710773 | — |
| Reactant | 2-Methanesulfinyl-7-(2-methoxy-phenyl)-pyrrolo[2,1-f][1,2,4]triazine | HCID 66710791 | — |
| Product | HCID 66711761 | HCID 66711761 | — |
Reaction Steps
The compound was made in an analogous fashion to Example 322 replacing 2-Methanesulfinyl-7-(2-methoxy-phenyl)-pyrrolo[2,1-f][1,2,4]triazine with 7-(3-Chloro-phenyl)-2-methanesulfinyl-pyrrolo[2,1-f][1,2,4]triazine to afford 90.14 mg of 1-[7-(3-Chloro-phenyl)-pyrrolo[2,1-f][1,2,4]triazin-2-yl]-1H-imidazo[4,5-c]pyridine as a lyophilized powder. (M+H)=347.6. 1H NMR (400 MHz, DMSO, d6) δ 9.42 (s, 1H), 9.21 (s, 1H), 8.61 (m, 1H), 8.53 (m, 1H), 8.35 (m, 1H), 8.15 (m, 1H), 7.63 (m, 4H), 7.36 (d, 1H, J=4.89 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08471005B2 |
| Source dataset | uspto-grants-2013_06 |
| ORD ID | ord-298509c1bcc84a48bb66750609cf9371 |
| Source note | uspto-grants-2013_06 |