Trifluoromethanesulfonate → HCID 66712674, compound

Participants

Role	Name	HCID	Charge
Reactant	Trifluoromethanesulfonate	HCID 2758875	—
Reactant	3-(2-Morpholin-4-ylethoxy)aniline	HCID 6486616	—
Reactant	N-tert-Butyl-3-(2-methanesulfinyl-pyrrolo[2,1-f][1,2,4]triazin-7-yl)-benzenesulfonamide	HCID 66711063	—
Product	HCID 66712674	HCID 66712674	—

Reaction Steps

Prepared by following a procedure analagous to Example 251c by using 3-(2-Morpholin-4-yl-ethoxy)-phenylamine and N-tert-Butyl-3-(2-methanesulfinyl-pyrrolo[2,1-f][1,2,4]triazin-7-yl)-benzenesulfonamide as a triflate salt. 1H-NMR (DMSO) δ 9.9 (br s, 1H), 9.6 (s, 1H), 9.15 (s, 1H), 8.5 (s, 1H), 8.4 (d, J=8.0 Hz, 1H), 7.9 (d, J=8.0 Hz, 1H), 7.75 (m, 1H), 7.6 (s, 1H), 7.55 (d, J=8.3 Hz, 1H), 7.3 (m, 2H), 7.2 (d, J=4.7 Hz, 1H), 7 (d, J=4.7 Hz, 1H), 6.7 (d, J=10.4 Hz, 1H), 4.3-3.3 (m, 12H), 1.1 (s, 9H); LC/MS (ESI+): 551 (M+H).

Provenance & Evidence

DOI	10.6084/m9.figshare.5104873.v1
Patent number	US08471005B2
Source dataset	uspto-grants-2013_06
ORD ID	ord-5cbfdb9e380846ffb84e18ca8ecc8b29
Source note	uspto-grants-2013_06