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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1262534Generated: November 3, 2026

Triethylamine → HCID 12796234, compound

https://huagongshe.com/reaction/1262534

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTriethylamineHCID 8471—
ReactantDicyclohexylcarbodiimideHCID 10868—
ReactantAlclofenacHCID 30951—
ReactantGlycine ethyl ester, hydrochlorideHCID 2723640—
SolventChloroformHCID 6212—
SolventTetrahydrofuranHCID 8028—
ProductHCID 12796234HCID 12796234—

Reaction Steps

4-Allyloxy-3-chloro-phenylacetic acid (4.3 g) was dissolved in dry tetrahydrofuran (20 ml). To the solution was added glycine ethyl ester hydrochloride (2.85 g) in dry chloroform (30 ml) containing dry triethylamine (2.8 ml). DCC (4.1 g) was added and the reaction mixture was stirred overnight at room temperature.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04452783
Source datasetuspto-grants-1984_06
ORD IDord-f5f8b8a4323f46f5a2edcb9764036443
Source noteuspto-grants-1984_06