HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isocyanate → HCID 13320288, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isocyanate | HCID 8022 | — |
| Reactant | HCID 13320286 | HCID 13320286 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 13320288 | HCID 13320288 | — |
Reaction Steps
A mixture of 7.3 g. of trans 4-(2-allylphenoxy)-1-ethyl-3-pyrrolidinol and 2.5 g. of ethylisocyanate in 30 ml. of benzene was stirred for 48 hr. The benzene was replaced by petroleum ether and the solution chilled. The yield of precipitate melting at 53-6° C. was 78%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04452809 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-3e31cf70295f4c80bba160b667277565 |
| Source note | uspto-grants-1984_06 |