HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium Carbonate → HCID 12289429, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium Carbonate | HCID 517111 | — |
| Reactant | Benzenecarboximidic acid, 3-acetyl-, ethyl ester, hydrochloride | HCID 12289426 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12289429 | HCID 12289429 | — |
Reaction Steps
A mixture of 14 g. (0.08 mole) of 3-acetylbenzenecarboximidic acid ethyl ester, hydrochloride of A. above and 14 g. (0.15 mole) of finely ground ammonium carbonate in 100 ml. of ethanol is heated at boiling temperature in an open flask for 3 hours. The solution is cooled and the first small amount of precipitate is collected and is discarded. The filtrate is further cooled to precipitate 6.7 g. of product with a melting point of 193° (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04452985 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-6bad46dd373641b885812a09cba79cd1 |
| Source note | uspto-grants-1984_06 |