HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 13073691, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,6-Dichloro-4-nitropyridine | HCID 3841070 | — |
| Reactant | HCID 54506707 | HCID 54506707 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 13073691 | HCID 13073691 | — |
Reaction Steps
Quantities of 19.3 gm (0.1 mol) of 2,6-dichloro-4-nitropyridine and 23.1 gm (0.11 mol) of 2,5-dichloro-4-methylmercaptophenol were dissolved in 100 ml of acetone, 13.8 gm (0.1 mol) of K2CO3 were added, and the resulting mixture was stirred for 3 hours under reflux. It was then stirred into 500 ml of water, and the precipitate formed was recovered by suction filtration.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04453972 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-1feb865e8d6c4138848c6fd5fd34c49c |
| Source note | uspto-grants-1984_06 |