3-Pyridinecarbonyl chloride, hydrochloride (1:1) → 2,2,8,8-Tetramethylnonane-1,9-diyl dipyridine-3-carboxylate

HRID 1262823Notes

Reaction equation

HRID 1262823 reaction equation
Cl.[C:2](Cl)(=[O:9])[C:3]1[CH:8]=[CH:7][CH:6]=[N:5][CH:4]=1.[CH3:11][C:12]([CH3:25])([CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][C:20]([CH3:24])([CH3:23])[CH2:21][OH:22])[CH2:13][OH:14]>N1C=CC=CC=1>[C:2]([O:22][CH2:21][C:20]([CH3:24])([CH3:23])[CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][C:12]([CH3:25])([CH3:11])[CH2:13][O:14][C:2](=[O:9])[C:3]1[CH:8]=[CH:7][CH:6]=[N:5][CH:4]=1)(=[O:9])[C:3]1[CH:8]=[CH:7][CH:6]=[N:5][CH:4]=1

Participants

4

Reactant 2

HCID 884383-Pyridinecarbonyl chloride, hydrochloride (1:1)HCID 30696741,9-Nonanediol, 2,2,8,8-tetramethyl-

Product 1

HCID 30696752,2,8,8-Tetramethylnonane-1,9-diyl dipyridine-3-carboxylate

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

106.2 Grams (0.6 mole) of nicotinoyl chloride hydrochloride in 300 ml of anhydrous pyridine were reacted with 21.6 grams (0.1 mole) of 2,2,8,8-tetramethyl-1,9-nonanediol according to the procedure described in the above example.

Sources & evidence

ORD record
ord-c0eab6f4676e4f1d916b4259afd77d83
Source dataset
uspto-grants-1984_06
Patent number
US04454145

Reaction notes

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