HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Pyridinecarbonyl chloride, hydrochloride (1:1) → 2,2,8,8-Tetramethylnonane-1,9-diyl dipyridine-3-carboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Pyridinecarbonyl chloride, hydrochloride (1:1) | HCID 88438 | — |
| Reactant | 1,9-Nonanediol, 2,2,8,8-tetramethyl- | HCID 3069674 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | 2,2,8,8-Tetramethylnonane-1,9-diyl dipyridine-3-carboxylate | HCID 3069675 | — |
Reaction Steps
106.2 Grams (0.6 mole) of nicotinoyl chloride hydrochloride in 300 ml of anhydrous pyridine were reacted with 21.6 grams (0.1 mole) of 2,2,8,8-tetramethyl-1,9-nonanediol according to the procedure described in the above example.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04454145 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-c0eab6f4676e4f1d916b4259afd77d83 |
| Source note | uspto-grants-1984_06 |