HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 11615198, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 13320105 | HCID 13320105 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11615198 | HCID 11615198 | — |
Reaction Steps
(Z)-1-Fluoro-2-phenyl-3-phthalimidopropene (0.25 g) is treated with hydrazine hydrate (50 mg) in ethanol (2 ml), and then concentrated hydrochloric acid (2 ml) and water (2 ml). Recrystallization of the resulting product (0.19 g) from ethanol/ether affords pure (Z)-2-phenyl-3-fluoroallylamine, as the hydrochloride: m.p. 145°;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04454158 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-5c253bfea547459f93205d6492117d5e |
| Source note | uspto-grants-1984_06 |