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HRID1263058

反应详情

EQUATION

反应方程式

HRID 1263058 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)CC(=O)Cl
HCID81514

Butanoyl chloride, 3,3-dimethyl-

C6H11ClO

结构：NNC1=Nc2ccc(Br)cc2C(c2ccccc2)=NC1
HCID12570862

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)Cc1nnc2n1-c1ccc(Br)cc1C(c1ccccc1)=NC2
HCID13343346

未命名化合物

PROCEDURE

实验过程

Following the procedure of Example 5, 2.0 g of 7-bromo-2-hydrazino-5-phenyl-3H-1,4-benzodiazepine is reacted with 1.01 ml of tert-butyl acetylchloride to yield 1.17 g of title product with melting point 229.5°-232° C. and 0.30 g of title product with melting point 205°-219° C.