HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Phenylmaleimide → HCID 13547662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Phenylmaleimide | HCID 13662 | — |
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 13547662 | HCID 13547662 | 48% |
Reaction Steps
The procedure of Example 1 is repeated using 10 grams of 2,6-di-tert-butyl-4-mercaptophenol, 7.26 grams of N-phenyl maleimide, and 0.73 grams of triethylamine. The residue is recrystallized from isopropanol to give 2.3 grams (48% yield) of white solid, m.p. 134°-137° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04456716 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-afb00246594b4b449bc2077028d30695 |
| Source note | uspto-grants-1984_06 |