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HRID1263305

反应详情

EQUATION

反应方程式

HRID 1263305 的结构方程式

REACTANTS

反应物

2
反应SMILES：O=C1C=CC(=O)N1c1ccccc1
HCID13662

N-Phenylmaleimide

C10H7NO2

反应SMILES：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

PRODUCTS

产物

1
反应SMILES：CC(C)(C)c1cc(SC2CC(=O)N(c3ccccc3)C2=O)cc(C(C)(C)C)c1O
HCID13547662

未命名化合物

收率 48%

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 10 grams of 2,6-di-tert-butyl-4-mercaptophenol, 7.26 grams of N-phenyl maleimide, and 0.73 grams of triethylamine. The residue is recrystallized from isopropanol to give 2.3 grams (48% yield) of white solid, m.p. 134°-137° C.

WORKUP

后处理

  1. customThe residue is recrystallized from isopropanol