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HRID1263306

反应详情

EQUATION

反应方程式

HRID 1263306 的结构方程式

REACTANTS

反应物

2
结构：O=C1C=CC(=O)N1c1ccccc1
HCID13662

N-Phenylmaleimide

C10H7NO2

结构：Cc1cc(S)cc(C(C)(C)C)c1O
HCID13547656

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc(SC2CC(=O)N(c3ccccc3)C2=O)cc(C(C)(C)C)c1O
HCID13547663

未命名化合物

收率 89%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 9.82 grams of 2-tert-butyl-6-methyl-4-mercaptophenol, 8.66 grams of N-phenylmaleimide, and 0.5 grams of triethylamine. The residue is recrystallized from a heptane-toluene mixture to give 16.44 grams of a white solid, m.p. 158°-160° C.

WORKUP

后处理

  1. customThe residue is recrystallized from a heptane-toluene mixture