HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-mercaptophenol → N-Dodecyl-2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-mercaptophenol | HCID 70370 | — |
| Reactant | 1H-Pyrrole-2,5-dione, 1-dodecyl- | HCID 87191 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | N-Dodecyl-2-(3,5-di-tert-butyl-4-hydroxyphenylthio)succinimide | HCID 13547659 | 39.7% |
Reaction Steps
The procedure of Example 1 is repeated using 13.27 grams N-dodecylmaleimide, 11.92 grams 2,6-di-tert-butyl-4-mercaptophenol, and 0.5 grams triethylamine. The sample is purified by dry column chromatography to give 10.0 grams of a clear syrup.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04456716 |
| Source dataset | uspto-grants-1984_06 |
| ORD ID | ord-8ae647199b6c4548bef611eacc01a282 |
| Source note | uspto-grants-1984_06 |