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HRID1263310

反应详情

EQUATION

反应方程式

HRID 1263310 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

结构：CCCCCCCCCCCCN1C(=O)C=CC1=O
HCID87191

1H-Pyrrole-2,5-dione, 1-dodecyl-

C16H27NO2

PRODUCTS

生成物

1
结构：CCCCCCCCCCCCN1C(=O)CC(Sc2cc(C(C)(C)C)c(O)c(C(C)(C)C)c2)C1=O
HCID13547659

未命名化合物

收率 39.7%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 13.27 grams N-dodecylmaleimide, 11.92 grams 2,6-di-tert-butyl-4-mercaptophenol, and 0.5 grams triethylamine. The sample is purified by dry column chromatography to give 10.0 grams of a clear syrup.

WORKUP

后处理

  1. customThe sample is purified
  2. customby dry column chromatography