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HRID1263311

反应详情

EQUATION

反应方程式

HRID 1263311 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)c1cc(S)cc(C(C)(C)C)c1O
HCID70370

2,6-Di-tert-butyl-4-mercaptophenol

C14H22OS

结构：O=C1C=CC(=O)N1C1CCCCC1
HCID74203

1H-Pyrrole-2,5-dione, 1-cyclohexyl-

C10H13NO2

PRODUCTS

生成物

1
结构：CC(C)(C)c1cc(SC2CC(=O)N(C3CCCCC3)C2=O)cc(C(C)(C)C)c1O
HCID13547661

未命名化合物

收率 50.3%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

The procedure of Example 1 is repeated using 11.95 grams of 2,6-di-tert-butyl-4-mercaptophenol, 8.96 grams of N-cyclohexylmaleimide, and 0.5 grams of triethylamine. The residue is recrystallized from a heptane-toluene mixture to give 10.5 grams of a white solid, m.p. 94°-98° C.

WORKUP

后处理

  1. customThe residue is recrystallized from a heptane-toluene mixture