HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 18617416, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 12052638 | HCID 12052638 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 18617416 | HCID 18617416 | 89% |
Reaction Steps
To the benzyl amine (Example 4, Part A; 20 mg, 0.03 mmol) was added 6 N HCl (1 mL) and the mixture stirred at room temperature for 1 h. The solution was diluted with 5 mL of H2O, washed with Et2O, and the aqueous layer concentrated under reduced pressure; yielding 17 mg (89%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541499B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-001ae290f6544dd48a0e3d92574081be |
| Source note | uspto-grants-2003_04 |