HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 18618216, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Methyl 3-amino-4-methylthiophene-2-carboxylate | HCID 123584 | — |
| Solvent | 1-Butanol | HCID 263 | — |
| Product | HCID 18618216 | HCID 18618216 | — |
Reaction Steps
A solution of methyl 3-amino-4-methyl-2-thenoate (25 g) and hydrazine hydrate (20 ml) in butanol (150 ml) was heated under reflux for 18 hours. On cooling the solvent was removed and teh residue was recrystallised from toluene to give the title product, m.p. 141-143° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541630B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-eb84bb2ec50947fca003ae0fc60f3ea0 |
| Source note | uspto-grants-2003_04 |