HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 18617583, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | HCID 18617551 | HCID 18617551 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 18617583 | HCID 18617583 | — |
Reaction Steps
40 mg (0.09 mmol) of 4-(4-amino-piperidin-1-yl)-N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-benzamide. (reference Example 1aav). was dissolved in 2 ml of pyridine, 22 mg (0.22 mmol) of acetic anhydride was added and stirred at room temperature for 16 h. The reaction mixture was evaporated to dryness. MS (CI) 430 (M+H)+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06541505B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-ecc14c0e40b54b2ba36f020d2fb46a28 |
| Source note | uspto-grants-2003_04 |