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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1264326Generated: October 31, 2026

Acetic Anhydride → HCID 18617583, compound

https://huagongshe.com/reaction/1264326

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAcetic AnhydrideHCID 7918—
ReactantHCID 18617551HCID 18617551—
SolventPyridineHCID 1049—
ProductHCID 18617583HCID 18617583—

Reaction Steps

40 mg (0.09 mmol) of 4-(4-amino-piperidin-1-yl)-N-[2-(3-Cyano-1H-indol-5-yl)-ethyl]-benzamide. (reference Example 1aav). was dissolved in 2 ml of pyridine, 22 mg (0.22 mmol) of acetic anhydride was added and stirred at room temperature for 16 h. The reaction mixture was evaporated to dryness. MS (CI) 430 (M+H)+.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06541505B1
Source datasetuspto-grants-2003_04
ORD IDord-ecc14c0e40b54b2ba36f020d2fb46a28
Source noteuspto-grants-2003_04