Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | P-Cresol | HCID 2879 | — |
| Reactant | 2,2,2-Trifluoro-1,1-ethanediol | HCID 67901 | — |
| Product | HCID 9839430 | HCID 9839430 | — |
Reaction Steps
5.8 g (50 mmol) of p-cresol and 15.5 g (100 mmol) of 75% fluoral hydrate are introduced into a 100 ml reactor. 5 g of MgO are added. The mixture is heated at 105° C. for 8 hours. After treating according to the protocol described in Example 1, 70% of dihydroxyalkylated product are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06541674B2 |
|---|
| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-46e55bb80a1e48e386306b47c3c87c93 |
|---|
| Source note | uspto-grants-2003_04 |
|---|
