Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | 2,2,2-Trifluoro-1,1-ethanediol | HCID 67901 | — |
| Product | HCID 10220179 | HCID 10220179 | 45% |
Reaction Steps
12.5 g (100 mmol) of p-chlorophenol and 3.9 g (25 mmol) of 75% fluoral hydrate are introduced into a 100 ml reactor. 6 g of hydrotalcite Mg6AlGa(O4)16.4H2O are added and the mixture is heated at 100° C. for 7 hours. After treating the reaction medium according to the protocol described in Example 1, a yield of 45% of the expected product is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06541674B2 |
|---|
| Source dataset | uspto-grants-2003_04 |
|---|
| ORD ID | ord-9b9e601f333741c58e8bfd9c00b364a5 |
|---|
| Source note | uspto-grants-2003_04 |
|---|
