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HRID1264926

反应详情

EQUATION

反应方程式

HRID 1264926 的结构方程式

REACTANTS

反应物

2
结构：COC(=O)c1ccc(C(N)=O)cc1
HCID596094

methyl 4-carbamoylbenzoate

C9H9NO3

结构：O=C(CBr)c1cc(C(F)(F)F)cc(C(F)(F)F)c1
HCID2736170

1-[3,5-Bis(trifluoromethyl)phenyl]-2-bromoethan-1-one

C10H5BrF6O

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(-c2nc(-c3cc(C(F)(F)F)cc(C(F)(F)F)c3)co2)cc1
HCID18613896

未命名化合物

收率 24%

PROCEDURE

实验过程

In the same manner as in Example 1, methyl 4-carbamoylbenzoate was reacted with 3,5-bis(trifluoromethyl)phenacyl bromide to obtain methyl 4-[4-[3,5-bis(trifluoromethyl)phenyl]-2-oxazolyl]benzoate. The product was. recrystallized from ethanol., Yield: 24%. Pale yellow prisms. Melting Point: 180 to 181° C.