HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionicotinamide → HCID 18613883, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionicotinamide | HCID 737155 | — |
| Reactant | Ethyl 4-(2-bromoacetyl)benzoate | HCID 11966043 | — |
| Product | HCID 18613883 | HCID 18613883 | 67% |
Reaction Steps
In the same manner as in Example 28, thionicotinamide was reacted with ethyl 4-bromoacetylbenzoate to obtain ethyl 4-[2-(3-pyridyl)-4-thiazolyl]benzoate hydrobromide. The product was recrystallized from ethanol. Yield: 67%. Pale yellow prisms. Melting point: 234 to 236° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06545009B1 |
| Source dataset | uspto-grants-2003_04 |
| ORD ID | ord-8d94ae42f12d40409bc6a634193b7d52 |
| Source note | uspto-grants-2003_04 |