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HRID1264934

反应详情

EQUATION

反应方程式

HRID 1264934 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(C(=O)CBr)cc1
HCID69272

2-Bromo-4'-methylacetophenone

C9H9BrO

结构：COC(=O)c1ccc(C(N)=S)cc1
HCID11401319

Methyl 4-carbamothioylbenzoate

C9H9NO2S

PRODUCTS

生成物

1
结构：COC(=O)c1ccc(-c2nc(-c3ccc(C)cc3)cs2)cc1
HCID18613871

未命名化合物

收率 61%

PROCEDURE

实验过程

In the same manner as in Example 28, methyl 4-thiocarbamoylbenzoate was reacted with 4-methylphenacyl bromide to obtain methyl 4-[4-(4-methylphenyl)-2-thiazolyl]benzoate. The product was recrystallized from ethanol. Yield: 61%. Pale yellow prisms. Melting point: 185 to 187° C.